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Title
Statistics in the Laboratory: A New American Laboratory Column
Friday, September 25, 2015
Stanley N. Deming
Welcome to “Statistics in the Laboratory.” This column will appear four times a year and will build on the popular “Statistics in Analytical Chemistry” series by David Coleman and Lynn Vanatta ...
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Five Ways to Improve the Workflow and Financial Health of the Laboratory
Friday, September 25, 2015
Trish Meek
Henry Ford quipped, “There are no big problems; there are just a lot of little problems.”
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Recent Advances in ICP Spectrometers
Monday, September 28, 2015
Mark Grey
When SPECTRO Analytical Instruments (Kleve, Germany) sought to redesign its inductively coupled plasma (ICP) spectrometer instrument line, the company’s engineers worked to address some very specific ...
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Statistics in the Laboratory: Control Charts, Part 1
Tuesday, January 26, 2016
Stanley N. Deming
Statistical process control (SPC) charts were introduced briefly in the previous column (October 2015).
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Computer-Assisted Structure Elucidation in Routine Analysis
Tuesday, January 26, 2016
Patrick Wheeler
Steve Hayward
Mikhail Elyashberg
The elucidation of unknown structures, especially those with novel moieties found in natural products, often results in initially incorrect published structures, which then require either exhaustive ...
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Determination of Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography and Pulsed Flame Photometric Detection
Friday, February 19, 2016
Cynthia Elmore
Michael Duffy
The carbonated beverage and petrochemicals industries are just some areas in which the analysis of volatile sulfur-containing compounds in process streams is a critical quality-control step.
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Ion-Exchange Selectivity and High-Resolution Accurate-Mass Spectrometry Elucidate Lithium-Ion Battery Degradation Pathways
Monday, May 09, 2016
Christopher Pohl
Charanjit Saini
Rosanne W. Slingsby
Paul J. Voelker
Kate Comstock
John Moote
Michael P. Balogh
Ramona Y. Ying
Improved performance and lifetime of lithium-ion batteries is important for automobile manufacturers that produce cars powered electrochemically by lithium-ion battery packs.
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High-Speed Zone Refining
Thursday, June 16, 2016
Julie DeCook
Zone refining is a process in which organic and inorganic compounds are purified.
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Selecting a GC Inlet Liner
Tuesday, July 26, 2016
Linx Waclaski
Introduction of gas chromatography samples typically occurs through a heated inlet containing a glass liner.
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Automating Solvent Removal From Winterized Cannabis Oil Extract
Wednesday, August 31, 2016
Alison Wake
Jim Bilotta
A centrifugal evaporator is compared to a rotary evaporator for the batch concentration of winterized cannabis extract in ethanol.
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High-Pressure Ion Chromatography Enables Fast, Reliable Analysis of Inorganic Cations and Ammonium in Environmental Water Samples
Thursday, September 01, 2016
Carl Fisher
Common alkali and alkaline earth cations are not considered primary drinking water contaminants, but alkaline water can potentially interfere with water clarification and disinfection procedures and ...
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Automated Chromatographic Solid-Phase Extraction Using an Autosampler
Thursday, September 01, 2016
Mark Hayward
Jonathan Ho
Rick Youngblood
Matthew T. Hardison
Tom Moran
Kim Gamble
Solid-phase extraction (SPE) is a preferred tool for isolating target analytes from complex matrices because the availability of a diverse range of chromatographic sorbents enables targeted approaches...
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Automated Liquid Chromatography Method Development Design and Practice
Thursday, September 01, 2016
Gary W. Yanik
Method development bottlenecks can be minimized with good planning, setup, procedures and techniques.
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Considerations for Diffuse Reflection Spectroscopy
Thursday, September 01, 2016
Stacey Carrier
Reflected light allows us to perceive the world around us.
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Comparative QC Test Methods for Toothpaste Consistency
Tuesday, September 27, 2016
Robert McGregor
Important quantitative data can be obtained in the study of viscosity by measuring the consistency of toothpaste, i.e., thickness, ease of handling and ability to retain position, and observing the ...
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Statistics in the Laboratory: The Capability of a Measurement Process
Tuesday, September 27, 2016
Stanley N. Deming
Measurement processes must be fit for use. In this column, we’ll develop some quantitative statistical descriptors of the capability of a measurement process to be valid for its intended purpose.
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Urinary Drug Testing: Small Changes for Big Improvements in Sensitivity
Tuesday, September 27, 2016
Jenny Cybulski
An oversight or mistake in drug testing can have dire consequences—a positive drug test can ruin the possibility of employment, turn an accident into a lawsuit, or cause a physician to discontinue ...
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Closing the Consumption Gap: Making GC More Accessible
Friday, November 04, 2016
Eric Denoyer
Paul Deitrick
Gas chromatography users agree on at least two things: that GC is a mature technology, and that the performance and features of instrumentation largely meet the application requirements for which GC ...
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Comparison of Crystallization Behavior of Different-Colored Polypropylene Parts Using a Single DSC Experiment
Friday, January 20, 2017
James A. Browne
A compositional analysis may explain the reasons for variations in processing behavior, but is time consuming and expensive. As an alternative, straightforward differential scanning calorimetry (DSC) ...
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High-Throughput VOC and Inorganic Gas Analysis: Automated SIFT-MS
Friday, January 20, 2017
Mark J. Perkins
Vaughan S. Langford
Murray J. McEwan
A sensitive technique called selected ion flow tube mass spectrometry (SIFT-MS) allows the direct, real-time monitoring of inorganic gases and volatile organic compounds (VOCs), with no need to ...
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